N-Isopropylbenzylamine CAS 102-97-6
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- Appearance: White powder
- Assay: 99. 0%min
- Stock: In stock
- Sample: Available
- Zhishang Chemical: N-Isopropylbenzylamine Supplement
N-Isopropylbenzylamine: The Complete Guide
Index of N-Isopropylbenzylamine Contents
N-Isopropylbenzylamine for Sale
Basic Info of N Isopropylbenzylamine
N Isopropylbenzylamine; Isopropylbenzylamine; N-Benzylisopropylamine; Benzylisopropylamine
API; Pharmaceutical raw materials; Organic raw materials
What is N-Isopropylbenzylamine?
N-isopropyl benzylamine is a compound that shows up in the chemical literature. It generally plays an intermediary function in experimental synthesis and the application of new natural change. Regardless of its minimal usage on record, it is popular that it drew in the interest of DEA due to its use as a diluent or replacement for methamphetamine by prohibited methamphetamine suppliers, and there were many recorded sightings between 2007 and also 2008.
As of 2018, DEA scientists pertaining to the methamphetamine evaluation program claimed that isopropyl benzylamine showed up only “periodically”, and also the program identified certain paths and other contaminations in taken drug examples. The substance is a chain isomer of methamphetamine and also has the very same chemical formula as well as molar mass, to ensure that its hydrochloride has comparable physical buildings, such as fairly close melting point and also similar look.
Isopropylbenzylamine itself is ruled out to have any kind of excitatory effects, although anecdotal reports suggest that it may be connected to adverse effects, such as migraine as well as complication, which are generally not related to methamphetamine itself. The poisoning of N-isopropyl benzylamine has not been researched.
- N-benzylisopropylamine is a typically made use of organic base as well as an important resources for natural synthesis.
- N-Isopropylbenzylamine forms amine adducts with ferrocene in toluene at ambient temperature.
- N-Isopropylbenzylamine is also used to synthesize N-benzylidene isopropylamine-n-oxide.
- Because n isopropylbenzylamine is similar to methamphetamine in appearance and physical properties, it has recently been considered by DEA.
- Utilizing n benzylisopropylamine as ligand, bis(cyclopentadienyl)magnesium was prepared and also identified.
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Application of N-Isopropylbenzylamine
In a 500 mL three-necked flask equipped with a thermostat, a constant-pressure going down funnel with a drying tube, and a magnetic stirrer, lithium aluminum hydride (4.5 g, 0.12 mol) was suspended in 150 mL of dry ice-salt bath cooled of tetrahydrofuran, stirring vigorously. The N-isopropylbenzamide was dissolved in dry tetrahydrofuran (200 ml) and transferred to a dropping funnel.
When the temperature of the system drops to below -5 ° C, slowly drop in the tetrahydrofuran solution dissolved with N-isopropylbenzamide, and the system releases heat immediately after dropping, and bubbles are released, adjust the dropping speed to make the reaction proceed smoothly. After the tetrahydrofuran solution of N-isopropylbenzamide was dripped, the reaction system was heated to reflux, and the reaction was maintained at reflux overnight. The reaction system was placed in an ice bath to cool down, and under vigorous stirring, a saturated ammonium chloride solution was slowly added.
After the saturated ammonium chloride solution was continuously added, no bubbles were generated. The insoluble matter in the system was filtered out, and ethyl acetate was used. The filter cake was washed several times and the filtrates were combined. The filtrate was placed in a separatory funnel and the layers were separated, and the aqueous layer was washed with ethyl acetate until it was no longer positive by TLC. The organic layers were combined and dried over anhydrous magnesium sulfate overnight. After drying, anhydrous magnesium sulfate was filtered off, and the filtrate was dried under reduced pressure. Purified by ethyl acetate/dichloromethane 3:1 system column chromatography to obtain 13.6 g of pure pale yellow liquid, yield 87%.
- N-Isopropylbenzylamine – PubChem
- [China Invention, China Invention Authorization] CN200810180203.8 Aramidothiazole derivatives and their preparation methods and uses
- N-BENZYLMETHYLAMINE HCL AND N-BENZYLETHYLAMINE HCL (“ICE” AND CRYSTAL METHAMPHETAMINE MIMICS) IN THE SOUTHWEST. Microgram Bulletin, August 2007