Valerophenone CAS 1009-14-9
Previous
Next
Factory Supply Valerophenone CAS 1009-14-9 with Best Price
- Appearance: Clear light yellow to yellow-green liquid
- Purity: 99. 0%min
- Stock: In stock
- Sample: Available
- Zhishang Chemical: Valerophenone Supplier & Manufacturer
Valerophenone: The Complete Guide
Valerophenone for Sale
Basic Info of Valerophenone
Basic Info
Chemical Name: | Valerophenone |
Other Name: | 1-Phenyl-1-pentanone; Pentanophenone; 1-Pentan-1-one; 1-Phenylpentan-1-one; Butyl phenone |
CAS: | 1009-14-9 |
EINECS: | 213-767-3 |
Type: | Food additives; Pharmaceutical raw materials; Flavor and Fragrance; Inorganic Salt |
Molecular Formula: | C11H14O |
Molecular Weight: | 162.23 |
Chemical Properties
Melting point | -9 °C |
Boiling point | 244-245 °C (lit.) |
density | 0.975 g/mL at 20 °C (lit.) |
refractive index | n20/D 1.5143(lit.) |
Fp | 217 °F |
storage temp. | Sealed in dry,Room Temperature |
form | Liquid |
color | Clear light yellow to yellow-green |
Specific Gravity | 0.98 |
Water Solubility | Insoluble in water. |
Stability: | Stable. Flammable. Incompatible with strong oxidizing agents, acids, bases, plastics. |
Other Info
Brand Name: | Zhishang Chemical |
Provide: | Valerophenone MSDS; Valerophenone COA |
What is Valerophenone?
Pentanone or butyl phenyl ketone is an aromatic ketone with the molecular formula C 6 h 5 C (o) C 4 H9. It is usually prepared by acylation of benzene with valeryl chloride.
Valerophenone is an organic intermediate, which can be prepared from benzene and n-valeryl chloride through Friedel-Crafts reaction, or from methyl benzoate through Grignard reaction.
Valerophenone Uses
- 1-Phenyl-1-pentanone can be made use of as natural synthesis intermediate as well as pharmaceutical intermediate, which can be used in laboratory r & d process and also chemical and also pharmaceutical synthesis procedure.
- Valerophenone is an organic chemical reagent that can be used in organic synthesis.
- Valerophenone is an organic intermediate, which can be prepared from benzene and n-valeryl chloride through Friedel-Crafts reaction, or from methyl benzoate through Grignard reaction.
- Pentanone is an aromatic ketone. It is used as a tool to study various photochemical processes 3. It is also an inhibitor of the enzyme carbonyl reductase 1. Pentanone is used as an intermediate of liquid crystal 2.
The Manager has Something to Say
This is William, CEO of Zhishang Chemical Co., Ltd.
Welcome to visit our factory . As the top chemical manufacturer, we have been striving for product quality, innovation , R&D, and customer service for the past 7 years. In the next 10 years or even longer, we are committed to becoming the most reliable chemical supplier in the world , creating a well-known international brand trusted by customers, with the spirit of “one meter wide, ten thousand meters deep”, we continue to focus on product research and development, continue to focus on customer service, continue to improve the supply chain service system, to create a professional chemical supply service team, to achieve win-win long-term cooperation. Please feel free to contact us if you have any questions.
Contact Us
- Email: sales002@sdzschem.com
- Phone: +86 176 5311 3209
- WhatsApp: +86 176 5311 3209
- WeChat: Zhishang17653113209
- Skype: +86 176 5311 3209
Facebook
Twitter
LinkedIn
Pinterest
Email
WhatsApp
If you want to buy valerophenone, pls contact us to get a free quote.
Preparation of Valerophenone
Report one
Add 156g benzene, 900mL dichloromethane and 146.5g anhydrous aluminum trichloride into a 2L three-necked flask, cool down to 0-5°C, slowly add 120.5g n-valeryl chloride dropwise, keep the internal temperature 0-10 °C. After the dropwise addition, the temperature was raised to 40 °C, and the reaction was stirred for 2 h. Under ice bath cooling, 500 mL of 1N hydrochloric acid solution was slowly added dropwise, and the solution was separated after the dropwise addition was completed. The aqueous phase was extracted with an additional 400 mL of DCM. After combining the organic phases, concentrate under reduced pressure and distill to obtain 142 g of valerophenone with a yield of 87%.- Report two
Dissolve 6.3 ml (0.05 mol) of methyl benzoate and 0.05 g of cuprous iodide in anhydrous tetrahydrofuran, and add dropwise 0.05 mol (diethyl ether solution prepared with 1.2 g of magnesium metal and a corresponding amount of n-butane bromide) Alkyl Grignard reagent, titrating Grignard reagent for about half an hour, and then reacting for about three hours to finally obtain 7.8 g of the target product, valerophenone, with a yield of 96%.
Reference
- Valerophenone – PubChem
- [China Invention, China Invention Authorization] CN200610041974.X Selective alkylation of acid anhydride or ester
- Milstein, D.; Stille, J. K. (1978). “A general, selective, and facile method for ketone synthesis from acid chlorides and organotin compounds catalyzed by palladium”. Journal of the American Chemical Society. 100 (11): 3636–3638. doi:10.1021/ja00479a077.
Valerophenone Supplier and Manufacturer
As a valerophenone supplier and manufacturer with a strict standard product quality system certificate, Zhishang Chemical has long been providing the best valerophenone raw materials to customers all over the world.
Over the years, relying on professional team experience and customer-centric team concept to meet customer needs in a timely manner, our company enjoys a high reputation in the world. At present, our company has served more than 6,000 customers and has established long-term cooperative relations with customers from many countries.
If you have a demand for valerophenone and related products, please contact our service staff Zhishang Chemical – White directly, and we will provide you with high-quality products at the best price.
Service
Pre-Sales Service
* Prompt reply and 24 hours online, professional team to provide the best price and high-quality product.
* Sample testing support.
* Every batch of products will be tested to ensure its quality.
* The packing also can be according to the customers` requirement.
* Any inquiries will be replied to within 24 hours.
* We provide a Commerical Invoices, Packing Lists, Bills of loading, COA, Health certificates, and Origin certificates. If your markets have any special requirements, let us know.
After-Sales Service
* The fact of logistics information monitoring.
* Any questions about the product can be consulted at any time.
* Product has any problem can return.
FAQ
Do you accept sample order?
We will make samples before mass production, and after the sample is approved, we’ll begin mass production. Doing 100% inspection during production, then doing random inspection before packing.
What’s your MOQ?
Our MOQ is 1kg. But usually we accept less quantities, such as 100g on the condition that the sample charge is 100% paid.
Is there a discount?
The different quantity has different discount.
HOW TO CONFIRM THE PRODUCT QUALITY BEFORE PLACING ORDERS?
You can get free samples for some products, you only need to pay the shipping cost or arrange a courier to us and take the samples. You can send us your product specifications and requests, we will manufacture the products according to your requests.
Do you supply product report?
Yes. We’ll give you product analysis report before shipping.
Shipping
1. ≤50kg, Express delivery recommended, usually called DDU service;
2. ≤500kg, Air shipping recommended, usually called FOB, CFR, or CIF service;
3. >500kg, sea shipping recommended, usually called FOB, CFR, or CIF service;
4. For high-value products, please select air shipping and express delivery for safe.
Quality Control of Valerophenone
Previous
Next
