CAS NO 121-32-4 ethyl vanillin

Basic Info

Model No.: CAS NO 121-32-4

Type: Fennel

CAS No.:: 121-32-4

MF: C9H10O3

MP:: 76 °C

Bp:: 285°C

MW:: 166.17400

FP:: 127°C

Refractive Index:: 1.434

Additional Info

Packaging: 225KG/drum

Productivity: 1000kg per Month

Brand: zhishang

Transportation: Ocean,Land,Air

Place of Origin: Shandong, China (Mainland)

Supply Ability: in stock

Certificate: ISO CE

HS Code: 121-32-4

Port: Shanghai,Tianjin,Qingdao

Product Description

From o-ethoxy phenol as raw materials from the system. This method is similar to vanillin process. Can also make o-ethoxy phenol and glyoxylate reaction, and then oxidized by copper oxide and aqueous caustic soda to form ethyl vanillin. Not only by saffron oil can produce vanillin, ethyl vanillin can also be produced. The safrole (4-allyl-1,2-methylenedioxybenzene) and potassium hydroxide in alcohol are heated in an autoclave to destroy the dioxygen ring. Then etherification was carried out by heating ethyl-sodium sulfate and the resultant 50% potassium hydroxide solution at 150-155 ° C for 2-3 hours. The etherified phenol mixture is dissolved in 50% ethanol, and then a small amount of sulfuric acid is added to reflux and heated to hydrolyze to form concentrated vanillin and isoeugenol. The former into a scale-like crystal precipitation, filtration, and then 50% ethanol recrystallization, that was pure. Dissolve the isoeugenol dissolved in 10% sodium hydroxide solution from the filtrate, and add the sodium nitrobenzene sulfonate to reflux for 3h. After cooling, acidify with dilute sulfuric acid to produce ethyl vanillin. Acid extraction with benzene generated oil, and then 35% sodium bisulfite solution, acidified and recrystallized to obtain the finished product.


Q1. Are you a manufacturer

Answer: Yes, we have our own factory called [ZhiShang Industry Group , we export by ShandongZhishangchemical Co., Ltd. 

Q2. Do you have GMP or DMF

Answer: Yes, we have GMP certificate for some products, and we can provide DMF as well.

Q3. What information should I let you know if I want to get a quotation

Answer: -Quality you require, eg. Assay, Purity, or single impurity

-Quantity you need

-Standard you want, such as USP, EP, JP etc.

Q4. How to make the payment

Answer: Escrow and T/T in advance are highly recommended. We can accept Western Union, Money Gram and Paypal as well

Q5. When will you deliver the goods

Answer: For sample(less than 1kg), in about 3 working days after payment; for larger orders (more than 1kg), in about 7 working days after payment. 

Q6. How will you deliver the goods

Answer: We have strong cooperation with DHL, TNT, UPS, FEDEX, EMS, China Air Post. For container products, we can do sea shipping.

You also can choose your own shipping forwarder.

Q7. When will we receive the goods

Answer: For samples, we will send by TNT/DHL/FEDEX/UPS express, usually it takes about 3-5 to reach you; for larger orders, it will take about 7 -10days at most. 

Q8. What if we find your products unsatisfied

Answer: We will send you a COA (Certificate of Analysis) to you first for you to confirm the quality, but if you find our products not confirm with the COA after you receive it, please show us your test result, we will refund you once we confirm that.

Product expansion

1> Cosmetic Raw Materials: Cosmetics is a variety of raw materials through a reasonable deployment of processing from the compound mixture. Cosmetics with a wide range of raw materials, different performance. According to the Raw Material properties and uses of cosmetics, can be divided into matrix materials and auxiliary raw materials in two categories.

2> Active Pharmaceutical Ingredients(API): API refers to the raw materials in the production of various types of preparations, which is the active ingredient in powder,crystal and paste for medicine use through chemical synthesis,plant extract, and preparations of biotechnology institute.

3> Fragrance And Spices: Spices are an important part of fine chemicals, it is composed of natural spices, synthetic spices and single fragrance.

4> Organic Raw Material: Intermediates are also known as organic intermediates. The use of coal tar or petroleum products as raw materials to produce dyes, resins, additives, and other intermediates.

5> Chemicals Used In Paints: Paint, the traditional Chinese name is paint. So-called coating is coated on the surface of the object that be protected or be adornment, and with the continuous film coating to form strong adhesion.

6> Pharmaceutical Intermediates: The so-called pharmaceutical intermediates, refers to the production of pharmaceutical products in the process, the use of raw materials, materials, accessories and other intermediate products.

7> Agricultural Chemicals: Research and agriculture related chemical, including pesticide, plant growth regulator, fertilizer, compound fertilizer, herbicide etc.



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